Magnetic tetraethylenepentamine modified multi-walled carbon nanotubes as matrix clean-up materials for organophosphorus pesticide residues analysis in cucumber
文献类型: 外文期刊
作者: Wang, Jun 1 ; Duan, Hui-Ling 1 ; Fan, Li 1 ; Lin, You-Ming 1 ; Sun, Jia-Ning 1 ; Zhang, Zhi-Qi 1 ;
作者机构: 1.Shaanxi Normal Univ, Sch Chem & Chem Engn, Key Lab Analyt Chem Life Sci Shaanxi Prov, Xian 710062, Peoples R China
2.Tibet Acad Agr & Anim Husb Sci, Inst Agr Prod Qual Stand & Testing Res, Lhasa 850032, Peoples R China
关键词: QuEChERS; Modified multi-wall carbon nanotubes; Magnetic adsorbent; Clean-up materials; Pesticide residues
期刊名称:FOOD CONTROL ( 影响因子:4.258; 五年影响因子:4.421 )
ISSN: 0956-7135
年卷期: 2021 年 124 卷
页码:
收录情况: SCI
摘要: In order to better remove the interfering substances in the vegetables, a type of tetraethylenepentamine modified multi-wall carbon nanotubes has been prepared. As-prepared materials contain amino-groups and organic chains, and magnetism is endowed by using physical blending method. Taking the magnetic tetraethylenepentamine modified multi-walled carbon nanotubes as matrix clean-up agents and combining with GC-MS, a modified QuEChERS method was established for the pesticide residues analysis in cucumber. The recoveries of 10 pesticide targets were 73.5%-114.2%, and the RSDs were between 4.9% and 18.6%, which could meet the requirements of food safety testing. Compared with the traditional clean-up materials, the prepared materials exhibited better clean-up performance while simplifying the pretreatment process. Given the excellent clean-up performance of the proposed materials, it was expected to be used in the clean-up process of other samples with complex contents.
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